3,3'-ureylene-di-(tert-butyl benzoate)

Base Information Edit

Chemical Name:3,3'-ureylene-di-(tert-butyl benzoate)
CAS No.:1070978-87-8
Molecular Formula:C₂₃H₂₈N₂O₅
Molecular Weight:412.486
Hs Code.:
Mol file:1070978-87-8.mol

Synonyms:3,3'-ureylene-di-(tert-butyl benzoate)

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Chemical Property of 3,3'-ureylene-di-(tert-butyl benzoate) Edit

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Technology Process of 3,3'-ureylene-di-(tert-butyl benzoate)

There total 3 articles about 3,3'-ureylene-di-(tert-butyl benzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 92146-82-2
tert-butyl 3-aminobenzoate

: 530-62-1
1,1'-carbonyldiimidazole

: 1070978-87-8
3,3'-ureylene-di-(tert-butyl benzoate)

Guidance literature:: In tetrahydrofuran; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/jm801245v

Reference yield:

: 58656-99-8
3-nitro-benzoic acid t-butyl ester

: 1070978-87-8
3,3'-ureylene-di-(tert-butyl benzoate)

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium on activated charcoal / methanol / 3.5 h

2: tetrahydrofuran / Heating / reflux

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;

Reference yield:

: 121-92-6
3-nitrobenzoic acid

: 1070978-87-8
3,3'-ureylene-di-(tert-butyl benzoate)

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 3 h / 0 - 20 °C

2: hydrogen / palladium on activated charcoal / methanol / 3.5 h

3: tetrahydrofuran / Heating / reflux

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;