{Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P)}⁽¹⁺⁾*(ClO₄)^(1-)=(Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P))(ClO₄)

Base Information

• Chemical Name: {Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P)}⁽¹⁺⁾*(ClO₄)^(1-)=(Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P))(ClO₄)
• CAS No.: 114347-54-5
• Molecular Formula: C₂₉H₃₆P₂RhS*ClO₄
• Molecular Weight: 680.974

Synonyms:{Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P)}⁽¹⁺⁾*(ClO₄)^(1-)=(Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P))(ClO₄)

Chemical Property of {Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P)}⁽¹⁺⁾*(ClO₄)^(1-)=(Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P))(ClO₄)

Chemical Property:

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Technology Process of {Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P)}⁽¹⁺⁾*(ClO₄)^(1-)=(Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P))(ClO₄)

There total 2 articles about {Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P)}⁽¹⁺⁾*(ClO₄)^(1-)=(Rh(C₈H₁₂)((CH₃)3PS)((C₆H₅)3P))(ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

bis(cyclooctadiene)rhodium(I) perchlorate (59420-05-2) + trimethylphosphane sulfide (2404-55-9) → {Rh(C8H12)((CH3)3PS)((C6H5)3P)}(1+)*(ClO4)(1-)=(Rh(C8H12)((CH3)3PS)((C6H5)3P))(ClO4) (114347-54-5)

Guidance literature:

With P(C₆H₅)3; In dichloromethane; N2 atmosphere; addn. of a slight excess of thio-compound and a stoich. amt. of phosphine to the complex in CH2Cl2;; pptn. by addn. of ether; ppt. was filtered off, washed with ether, and dried under vac.; elem. anal.;;

DOI:10.1016/S0277-5387(00)80891-8

Reference yield:

{Rh(C8H12)((CH3)3PS)2}(1+)*ClO4(1-)=(Rh(C8H12)((CH3)3PS)2)(ClO4) (114347-42-1) → {Rh(C8H12)((CH3)3PS)((C6H5)3P)}(1+)*(ClO4)(1-)=(Rh(C8H12)((CH3)3PS)((C6H5)3P))(ClO4) (114347-54-5)

Guidance literature:

With P(C₆H₅)3; In dichloromethane; N2 atmosphere; addn. of a stoich. amt. of phosphine to the complex in CH2Cl2;; pptn. by addn. of ether; ppt. was filtered off, washed with ether, and dried under vac.; elem. anal.;;

DOI:10.1016/S0277-5387(00)80891-8

upstream raw materials:

{Rh(C₈H₁₂)((CH₃)3PS)2}⁽¹⁺⁾*ClO₄^(1-)=(Rh(C₈H₁₂)((CH₃)3PS)2)(ClO₄)

bis(cyclooctadiene)rhodium(I) perchlorate

trimethylphosphane sulfide

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