N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide

Base Information

Chemical Name:N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide
CAS No.:118495-13-9
Molecular Formula:C₁₈H₂₁NO
Molecular Weight:267.371
Hs Code.:

Synonyms:N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide

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Chemical Property of N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide

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Technology Process of N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide

There total 4 articles about N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 129872-11-3
Crotonaldehyde benzylamine imine

: 118495-26-4
2-methyl-2-cyclopentene-1-carboxylic acid chloride

: 118495-13-9
N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide

Guidance literature:: With N,N-diethylaniline; In toluene; 1) -78 deg C, 2) warming up to room temperature overnight;
DOI:10.1021/jo00002a029

Reference yield:

: 118495-26-4
2-methyl-2-cyclopentene-1-carboxylic acid chloride

: 129872-11-3,63459-08-5
crotonaldehyde N-benzylimine

: 118495-13-9
N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide

Guidance literature:: With N,N-diethylaniline; In toluene; at -78 - 20 ℃; for 10h;
DOI:10.1021/jo00263a002

Reference yield:

: 100-46-9
benzylamine

: 118495-13-9
N-benzyl-N-1',3'-butadienyl-2-methyl-2-cyclopentene-1-carboxylic amide

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄ / diethyl ether / 2 h / 0 °C

2: C₆H₅NEt₂ / toluene / 10 h / -78 - 20 °C

With magnesium sulfate; N,N-diethylaniline; In diethyl ether; toluene;
DOI:10.1021/jo00263a002