phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside
CAS No.:876862-52-1
Molecular Formula:C₂₇H₄₆O₇SSi
Molecular Weight:542.81
Hs Code.:

Synonyms:phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

There total 1 articles about phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 13154-24-0
triisopropylsilyl chloride

: 263543-42-6
phenyl 3,4-O-(2’,3’-dimethoxybutane-2’,3’-diyl)-1-thio-α-D-mannopyranoside

: 876862-52-1
phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 7h;
DOI:10.1080/07328300500409150

Reference yield:

: 876862-52-1
phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

: 108-24-7
acetic anhydride

: phenyl 2-O-acetyl-3,4-O-(2’,3’-dimethoxybutane-2’,3’-diyl)-1-thio-6-O-triisopropylsilyl-α-D-mannopyranoside

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1055/s-0035-1560591

Reference yield:

: 876862-52-1
phenyl 6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

: 2-deoxy-6-O-triisopropylsilyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-2-phenylthio-β-D-glucopyranosyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Ag₂O; KI / CH₂Cl₂ / 11 h / Heating

2: NaN₃ / dimethylformamide / 15 h / 130 °C

With sodium azide; potassium iodide; silver(l) oxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/07328300500409150