Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

Base Information

Chemical Name:Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride
CAS No.:291306-21-3
Molecular Formula:C₁₈H₁₆Cl₂N₂*ClH
Molecular Weight:367.705
Hs Code.:

Synonyms:Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

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Technology Process of Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

There total 1 articles about Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 291306-20-2
(1S-cis )-4-(3,4-dichlorophenyl)-7-iodo-1,2,3,4-tetrahydro-N-methyl-1-naphthalenamine

: 557-21-1
dicyanozinc

: 291306-21-3
Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In DMF (N,N-dimethyl-formamide); at 100 ℃; for 3h;

Reference yield: 25.0%

: 291306-21-3
Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

: cis-(1S)-N-methyl-7-carboxamido-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

Guidance literature:: With sulfuric acid; at 100 ℃; for 1.16667h;

Reference yield:

: 291306-21-3
Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

: Cis-(1S)-N-methyl-7-(aminomethyl)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

Guidance literature:: Cis-(1S)-N-methyl-7-cyano-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 50 ℃; for 4h;

With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃;

With hydrogenchloride; In diethyl ether;