C₂₆H₃₈F₂O₅Si

Base Information

Chemical Name:C₂₆H₃₈F₂O₅Si
CAS No.:1369405-76-4
Molecular Formula:C₂₆H₃₈F₂O₅Si
Molecular Weight:496.667
Hs Code.:

C<sub>26</sub>H<sub>38</sub>F<sub>2</sub>O<sub>5</sub>Si

Synonyms:C₂₆H₃₈F₂O₅Si

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Chemical Property of C₂₆H₃₈F₂O₅Si

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Technology Process of C₂₆H₃₈F₂O₅Si

There total 9 articles about C₂₆H₃₈F₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1369405-75-3
(((2S,3R)-2,3-bis(benzyloxy)-4,4-difluorohex-5-en-1-yl)oxy)(tert-butyl)dimethylsilane

: 1369405-76-4
C₂₆H₃₈F₂O₅Si

Guidance literature:: With potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide; In water; acetone; at 20 ℃; for 48h;
DOI:10.1016/j.tetlet.2012.02.062

Reference yield:

: 1369405-71-9
(S)-2-((R)-1-(benzyloxy)-2,2-difluorobut-3-en-1-yl)oxirane

: 1369405-76-4
C₂₆H₃₈F₂O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 12 h / 130 °C

2.1: methanol; potassium carbonate / 8 h / 20 °C

3.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

4.2: 0 - 20 °C

5.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / water; acetone / 48 h / 20 °C

With methanol; dmap; potassium osmate(VI) dihydrate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; water; acetone; mineral oil;
DOI:10.1016/j.tetlet.2012.02.062

Reference yield:

: 1005768-69-3
(2R,3R)-3-O-benzyl-4,4-difluoro-5-hexene-1,2,3-triol

: 1369405-76-4
C₂₆H₃₈F₂O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: 12 h / 130 °C

4.1: methanol; potassium carbonate / 8 h / 20 °C

5.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

6.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

6.2: 0 - 20 °C

7.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / water; acetone / 48 h / 20 °C

With methanol; dmap; potassium osmate(VI) dihydrate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; methanesulfonyl chloride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; water; acetone; mineral oil;
DOI:10.1016/j.tetlet.2012.02.062