N-(6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-yl)-3-methoxybenzamide

Base Information

Chemical Name:N-(6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-yl)-3-methoxybenzamide
CAS No.:1384426-45-2
Molecular Formula:C₂₃H₂₅N₃O₂
Molecular Weight:375.47
Hs Code.:

Synonyms:N-(6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-yl)-3-methoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-yl)-3-methoxybenzamide

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Technology Process of N-(6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-yl)-3-methoxybenzamide

There total 2 articles about N-(6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-yl)-3-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1527-89-5
3-methoxybenzonitrile

: 1384426-35-0
6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-ol

: 1384426-45-2
N-(6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-yl)-3-methoxybenzamide

Guidance literature:: With sulfuric acid; acetic acid; at 60 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.tet.2012.05.074

Reference yield:

: 43102-70-1
6,6-dimethyl-1-phenyl-1,5,6,7-tetrahydro-4H-indazol-4-one

: 1384426-45-2
N-(6,6-dimethyl-1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-yl)-3-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 12 h / 20 °C / Inert atmosphere

2: sulfuric acid; acetic acid / 15 h / 60 °C / Inert atmosphere

With sodium tetrahydroborate; sulfuric acid; acetic acid; In ethanol; 2: Ritter reaction;
DOI:10.1016/j.tet.2012.05.074