sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate

Base Information

Chemical Name:sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate
CAS No.:1374853-98-1
Molecular Formula:C₂₃H₃₄NO₉*Na
Molecular Weight:491.514
Hs Code.:

Synonyms:sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate

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Chemical Property of sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate

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Technology Process of sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate

There total 3 articles about sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374853-99-2
C₃₂H₄₅NO₁₃

: 1374853-98-1
sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate

Guidance literature:: C₃₂H₄₅NO₁₃; With sodium methylate; In methanol;

With ammonium hydroxide; In methanol; for 2h;

In methanol; pH=6 - 7;

Reference yield:

: 145240-79-5
5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-1-(methoxycarbonyl)-D-glycero-α-D-galacto-2-nonulopyranosyl diethyl phosphite

: 1374853-98-1
sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.67 h / -40 °C

2.1: sodium methylate / methanol

2.2: 2 h

2.3: DOWEX-H resin / pH 6 - 7

With sodium methylate; trimethylsilyl trifluoromethanesulfonate; In methanol; acetonitrile;

Reference yield:

: 20298-34-4
methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-acetamido-α-D-glycero-D-galacto-2-nonulopyranosonate

: 1374853-98-1
sodium (3-methyl-5-phenylpentanyl-5-acetamido-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranoside)onate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C / Inert atmosphere

2.1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.67 h / -40 °C

3.1: sodium methylate / methanol

3.2: 2 h

3.3: DOWEX-H resin / pH 6 - 7

With sodium methylate; N-ethyl-N,N-diisopropylamine; trimethylsilyl trifluoromethanesulfonate; In methanol; acetonitrile;