(S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester

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Chemical Name:(S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester
CAS No.:191337-30-1
Molecular Formula:C₃₄H₃₈N₂O₇
Molecular Weight:586.685
Hs Code.:

Synonyms:(S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester

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Chemical Property of (S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester

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Technology Process of (S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester

There total 4 articles about (S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 191337-27-6
(S)-2-(3-Methyl-but-2-enylamino)-3-phenyl-propionic acid methyl ester

: (S)-3-Benzyloxycarbonylamino-3-fluorocarbonyl-propionic acid benzyl ester

: 191337-30-1
(S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester

Guidance literature:: With N-ethylmorpholine;; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4039(97)00726-0

Reference yield:

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 191337-30-1
(S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / NEt₃ / 6 h / Ambient temperature

2: 97 percent / K₂CO₃ / dimethylformamide / 3 h / Ambient temperature

3: 81 percent / PhSH, K₂CO₃ / dimethylformamide / 6 h / Ambient temperature

4: 80 percent / 4-ethyl morpholine / CH₂Cl₂ / 24 h / Ambient temperature

With N-ethylmorpholine;; potassium carbonate; thiophenol; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(97)00726-0

Reference yield:

: 870-63-3
prenyl bromide

: 191337-30-1
(S)-3-Benzyloxycarbonylamino-N-((S)-1-methoxycarbonyl-2-phenyl-ethyl)-N-(3-methyl-but-2-enyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / dimethylformamide / 3 h / Ambient temperature

2: 81 percent / PhSH, K₂CO₃ / dimethylformamide / 6 h / Ambient temperature

3: 80 percent / 4-ethyl morpholine / CH₂Cl₂ / 24 h / Ambient temperature

With N-ethylmorpholine;; potassium carbonate; thiophenol; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(97)00726-0