Technology Process of C27H42O4
There total 24 articles about C27H42O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 6h;
DOI:10.1271/bbb.130243
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.33 h / 0 - 20 °C
2.1: N,N-dimethyl-formamide / 0 - 20 °C
3.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C
3.2: 1 h / -78 - 20 °C
4.1: Dess-Martin periodane / dichloromethane / 0.25 h / 0 - 20 °C
5.1: aluminum amalgam; disodium hydrogenphosphate / methanol / 3 h / 0 - 20 °C
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 0 - 20 °C
With
disodium hydrogenphosphate; aluminum amalgam; n-butyllithium; carbon tetrabromide; tetrabutyl ammonium fluoride; Dess-Martin periodane; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1271/bbb.130243
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N,N-dimethyl-formamide / 0 - 20 °C
2.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C
2.2: 1 h / -78 - 20 °C
3.1: Dess-Martin periodane / dichloromethane / 0.25 h / 0 - 20 °C
4.1: aluminum amalgam; disodium hydrogenphosphate / methanol / 3 h / 0 - 20 °C
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 0 - 20 °C
With
disodium hydrogenphosphate; aluminum amalgam; n-butyllithium; tetrabutyl ammonium fluoride; Dess-Martin periodane;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1271/bbb.130243
