2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide

Base Information

Chemical Name:2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide
CAS No.:1422573-65-6
Molecular Formula:C₄₀H₅₀N₄O₂
Molecular Weight:618.863
Hs Code.:

Synonyms:2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide

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Technology Process of 2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide

There total 5 articles about 2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1422573-77-0
N-ethyl(4-hexyl)aniline

: 65739-39-1
2,2′-bipyridine-6,6′-dicarbonyl dichloride

: 1422573-65-6
2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 40 - 50 ℃;
DOI:10.1007/s11172-012-0124-4

Reference yield:

: 1077-16-3
hexylbenzene

: 1422573-65-6
2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / dichloromethane / Cooling with ice

2: acetic acid; sodium azide; sulfuric acid / 3 h / 60 - 70 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / Reflux

4: triethylamine / tetrahydrofuran / 40 - 50 °C

With aluminum (III) chloride; lithium aluminium tetrahydride; sodium azide; sulfuric acid; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; 2: |Schmidt Reaction;
DOI:10.1007/s11172-012-0124-4

Reference yield:

: 4479-74-7
2,2'-bipyridine-6,6'-dicarboxylic acid

: 1422573-65-6
2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 2.5 h / Reflux

2: triethylamine / tetrahydrofuran / 40 - 50 °C

With thionyl chloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1007/s11172-012-0124-4