N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone

Base Information

Chemical Name:N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone
CAS No.:1345512-85-7
Molecular Formula:C₂₂H₁₇ClN₄O₃S
Molecular Weight:452.921
Hs Code.:

Synonyms:N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone

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Chemical Property of N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone

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Technology Process of N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone

There total 4 articles about N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345512-95-9
C₁₇H₁₅ClN₂O₃S

: 90-02-8
salicylaldehyde

: 1345512-85-7
N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone

Guidance literature:: In butan-1-ol; at 110 ℃; for 12h;
DOI:10.1016/j.bmcl.2011.09.061

Reference yield:

: 899684-01-6
C₁₄H₁₄ClNO₂S

: 1345512-85-7
N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.5 h / 200 °C

2: potassium carbonate / acetone / 48 h / 55 °C

3: butan-1-ol / 12 h / 110 °C

With potassium carbonate; In acetone; butan-1-ol;
DOI:10.1016/j.bmcl.2011.09.061

Reference yield:

: 1082464-50-3
C₁₃H₉ClN₂OS

: 1345512-85-7
N'-[(2-hydroxyphenyl)methylene]-[4-oxo-5-(3-methyl-4-chlorophenyl)-thieno[2,3-d]pyrimidin-3(4H)-yl]acetohydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 48 h / 55 °C

2: butan-1-ol / 12 h / 110 °C

With potassium carbonate; In acetone; butan-1-ol;
DOI:10.1016/j.bmcl.2011.09.061