1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane

Base Information

• Chemical Name: 1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane
• CAS No.: 136213-56-4
• Molecular Formula: C₃₄H₂₁F₂₄IO₄
• Molecular Weight: 1076.4

Synonyms:1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane

Chemical Property of 1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane

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Technology Process of 1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane

There total 1 articles about 1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Martins sulfurane (32133-82-7) + 1-oxo-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane (136213-47-3) → 1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane (136213-56-4)

Guidance literature:

In dichloromethane; for 0.25h; Ambient temperature;

DOI:10.1021/jo00023a022

Reference yield:

1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane (136213-56-4) + trifluoroacetyl triflate (68602-57-3) → 1-(1-<2,2,2-trifluoro-1-phenyl-1-(trifluoromethyl)ethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octyl) trifluoromethanesulfonate (136213-58-6)

Guidance literature:

In chloroform-d1; for 5h; Ambient temperature;

DOI:10.1021/jo00023a022

Reference yield:

1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane (136213-56-4) + trifluoroacetic anhydride (407-25-0) → 1,1-bis(trifloroacetoxy)-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane (136213-53-1) + Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ5-ioda-3,5-dioxa-tricyclo[5.3.1.04,11]undeca-1(10),7(11),8-trien-4-yl ester (136213-59-7)

Guidance literature:

for 4h; Ambient temperature;

DOI:10.1021/jo00023a022

upstream raw materials:

Martins sulfurane

1-oxo-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane

Downstream raw materials:

1,1-bis(trifloroacetoxy)-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane

Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ⁵-ioda-3,5-dioxa-tricyclo[5.3.1.0^4,11]undeca-1(10),7(11),8-trien-4-yl ester

1-(1-<2,2,2-trifluoro-1-phenyl-1-(trifluoromethyl)ethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octyl) trifluoromethanesulfonate

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