ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate

Base Information

Chemical Name:ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate
CAS No.:1360546-37-7
Molecular Formula:C₂₈H₂₉NO₃
Molecular Weight:427.543
Hs Code.:

Synonyms:ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate

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Chemical Property of ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate

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Technology Process of ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate

There total 7 articles about ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: ethyl 2-(2-(dibenzylcarbamothioyl)-2,3-dihydro-1H-inden-1-yl)acetate

: 1360546-37-7
ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate

Guidance literature:: With trifluoroacetic anhydride; In dichloromethane; at 20 ℃; for 24h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/chem.201102332

Reference yield:

: 1360546-16-2
(E)-ethyl 3-(2-(3-(dibenzylamino)-3-thioxopropyl)phenyl)acrylate

: 1360546-37-7
ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: [Cu(acetonitrile)4]SbF₆; lithium 4-methoxyphenoxide; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tetrahydrofuran; N,N-dimethyl-formamide / -40 °C / Inert atmosphere

2: trifluoroacetic anhydride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With [Cu(acetonitrile)4]SbF₆; lithium 4-methoxyphenoxide; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201102332

Reference yield:

: 1360546-41-3
C₂₈H₂₉NO₃

: 1360546-37-7
ethyl 2-((1S,2R)-2-(dibenzylcarbamoyl)-2,3-dihydro-1H-inden-1-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: Lawessons reagent / tetrahydrofuran / 70 h / 20 °C

2: [Cu(acetonitrile)4]SbF₆; lithium 4-methoxyphenoxide; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tetrahydrofuran; N,N-dimethyl-formamide / -40 °C / Inert atmosphere

3: trifluoroacetic anhydride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With Lawessons reagent; [Cu(acetonitrile)4]SbF₆; lithium 4-methoxyphenoxide; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201102332