(E)-3-{6-[(tert-butyldimethylsilyl)oxy]hex-2-en-1-yl}-1-tosylpyrrolidine

Base Information

Chemical Name:(E)-3-{6-[(tert-butyldimethylsilyl)oxy]hex-2-en-1-yl}-1-tosylpyrrolidine
CAS No.:1353557-81-9
Molecular Formula:C₂₃H₃₉NO₃SSi
Molecular Weight:437.719
Hs Code.:

Synonyms:(E)-3-{6-[(tert-butyldimethylsilyl)oxy]hex-2-en-1-yl}-1-tosylpyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-{6-[(tert-butyldimethylsilyl)oxy]hex-2-en-1-yl}-1-tosylpyrrolidine

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Technology Process of (E)-3-{6-[(tert-butyldimethylsilyl)oxy]hex-2-en-1-yl}-1-tosylpyrrolidine

There total 2 articles about (E)-3-{6-[(tert-butyldimethylsilyl)oxy]hex-2-en-1-yl}-1-tosylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 277331-67-6
B-2-(E)-(5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-penteny-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1353557-81-9
(E)-3-{6-[(tert-butyldimethylsilyl)oxy]hex-2-en-1-yl}-1-tosylpyrrolidine

Guidance literature:: B-2-(E)-(5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-penteny-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; With N-(2-bromoethyl)-N-(2-propenyl)-4-methylbenzenesulfonamide; In tetrahydrofuran; pentane; at -78 - 0 ℃; for 1h;

B-2-(E)-(5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-penteny-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; With n-Undecane; dichloro{1,2-[bis(3,5-di-tert-butylpheny)phosphino-κP]benzene}iron(II); magnesium bromide; In tetrahydrofuran; pentane; at -78 - 0 ℃; for 24h; stereospecific reaction;
DOI:10.1021/jo202151f

Reference yield: 56.0%

: C₂₁H₄₄BO₃Si^(1-)*Li⁽¹⁺⁾

: 129748-56-7
N-(2-bromoethyl)-N-(2-propenyl)-4-methylbenzenesulfonamide

: 863418-78-4
N-allyl-N-ethyl-4-methyl-benzenesulfonamide

: 86553-37-9
3-methyl-1-tosylpyrrolidine

: 1353557-81-9
(E)-3-{6-[(tert-butyldimethylsilyl)oxy]hex-2-en-1-yl}-1-tosylpyrrolidine

Guidance literature:: With dichloro{1,2-[bis(3,5-di-tert-butylpheny)phosphino-κP]benzene}iron(II); magnesium bromide; In tetrahydrofuran; at 0 ℃; for 24h;
DOI:10.1021/jo202151f