C₆₈H₈₂N₂Si₃

Base Information

Chemical Name:C₆₈H₈₂N₂Si₃
CAS No.:1373216-35-3
Molecular Formula:C₆₈H₈₂N₂Si₃
Molecular Weight:1011.67
Hs Code.:

C<sub>68</sub>H<sub>82</sub>N<sub>2</sub>Si<sub>3</sub>

Synonyms:C₆₈H₈₂N₂Si₃

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Chemical Property of C₆₈H₈₂N₂Si₃

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Technology Process of C₆₈H₈₂N₂Si₃

There total 3 articles about C₆₈H₈₂N₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1373216-33-1
(4-iPrC₆H₄)3SiNH₂

: 18414-38-5
di(p-tolyl)dichlorosilane

: 1373216-35-3
C₆₈H₈₂N₂Si₃

Guidance literature:: (4-iPrC₆H₄)3SiNH₂; With n-butyllithium; In diethyl ether; hexane; at -35 ℃; for 3h; Inert atmosphere;

di(p-tolyl)dichlorosilane; In diethyl ether; hexane; at -35 - 20 ℃; Inert atmosphere;
DOI:10.1021/ic300495k

Reference yield:

: 1373216-32-0
tris(4-isopropylphenyl)silyl chloride

: 1373216-35-3
C₆₈H₈₂N₂Si₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium amide / tetrahydrofuran / Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / 3 h / -35 °C / Inert atmosphere

2.2: -35 - 20 °C / Inert atmosphere

With n-butyllithium; lithium amide; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/ic300495k

Reference yield:

: 586-61-8
4-iso-propylbromobenzene

: 1373216-35-3
C₆₈H₈₂N₂Si₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran / Inert atmosphere; Reflux

1.2: 48 h / -78 - 20 °C / Inert atmosphere; Reflux

2.1: lithium amide / tetrahydrofuran / Inert atmosphere

3.1: n-butyllithium / diethyl ether; hexane / 3 h / -35 °C / Inert atmosphere

3.2: -35 - 20 °C / Inert atmosphere

With n-butyllithium; lithium amide; magnesium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/ic300495k