((CH₃OC₆H₄NCCH₃)2)(CO)3Fe

Base Information

Chemical Name:((CH₃OC₆H₄NCCH₃)2)(CO)3Fe
CAS No.:65016-01-5
Molecular Formula:C₂₁H₂₀FeN₂O₅
Molecular Weight:436.247
Hs Code.:

((CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>NCCH<sub>3</sub>)2)(CO)3Fe

Synonyms:((CH₃OC₆H₄NCCH₃)2)(CO)3Fe

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Chemical Property of ((CH₃OC₆H₄NCCH₃)2)(CO)3Fe

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Technology Process of ((CH₃OC₆H₄NCCH₃)2)(CO)3Fe

There total 2 articles about ((CH₃OC₆H₄NCCH₃)2)(CO)3Fe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 109007-87-6
((C₅H₄N)2)((CH₃CH₂OCOCHCH)2)(CO)Fe

: 108895-04-1
(η2-diethyl muconate)(2,2'-bipyridyl)dicarbonyliron

: 65016-01-5
((CH₃OC₆H₄NCCH₃)2)(CO)3Fe

Guidance literature:: With carbon monoxide; In benzene; soln. of monocarbonyl compound was stirred at room temp. under CO 2-3 d, then concd. in vacuo beyond the crystallizaton point, crystalline residue was repeatedly washed with hexane; purified by crystallization from toluene or acetone; identified by elem. anal., IR and NMR spectra;

Reference yield:

: 108918-83-8
(η2-diethyl muconate){biacetyl bis(4-methoxyanil)}dicarbonyliron

: 82134-11-0
((CH₃OC₆H₄NCCH₃)2)((CH₃CH₂OCOCHCH)2)(CO)Fe

: 65016-01-5
((CH₃OC₆H₄NCCH₃)2)(CO)3Fe

Guidance literature:: In benzene; a partial disproportionation occurs on standing in soln.; products were not isolated; determined by IR spectra;

Reference yield: 68.0%

: 65016-01-5
((CH₃OC₆H₄NCCH₃)2)(CO)3Fe

: 624-49-7
dimethylfumarate

: 108895-11-0
(η2-dimethyl fumarate){biacetyl bis(4-methoxyanil)}dicarbonyliron

Guidance literature:: In benzene; Irradiation (UV/VIS); tricarbonyl complex was irradiated with ca. 5-fold excess of ligand for 1.5 h at 12-15°C under argon; solvent was removed, excess of ligand was sublimed; purified by crystallization from acetone; identified by elem. anal., IR, NMR and mass-spectra;