allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

Base Information

Chemical Name:allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside
CAS No.:1352813-68-3
Molecular Formula:C₄₆H₄₄O₁₆
Molecular Weight:852.846
Hs Code.:

Synonyms:allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

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Chemical Property of allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

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Technology Process of allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

There total 1 articles about allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 155835-94-2
allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

: methyl (3-O-acetyl-2,4-di-O-benzoyl-α-D-glucopyranosyl trichloroacetamidate)uronate

: 1352813-68-3
allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In toluene; at 0 - 4 ℃; for 48h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja2083015

Reference yield: 98.0%

: 1352813-68-3
allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

: 1352813-59-2
C₃₉H₄₀O₁₆

Guidance literature:: With pyridinium p-toluenesulfonate; In water; acetonitrile; at 80 ℃; for 36h;
DOI:10.1021/ja2083015

Reference yield:

: 1352813-68-3
allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

: 1352813-69-4
allyl [methyl(3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->3)-2,4,6-tri-O-benzoyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / water; acetonitrile / 36 h / 80 °C

2: pyridine / 3 h / -10 °C

With pyridine; pyridinium p-toluenesulfonate; In water; acetonitrile;
DOI:10.1021/ja2083015