5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole

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Chemical Name:5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole
CAS No.:1177558-02-9
Molecular Formula:C₁₃₂H₁₆₆FN₃O₆
Molecular Weight:1909.78
Hs Code.:

5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole

Synonyms:5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole

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Chemical Property of 5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole

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Technology Process of 5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole

There total 1 articles about 5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1177557-99-1
3,5-bis-[4-(2-ethylhexyloxy)phenyl]-1-iodo-4-methylbenzene

: 1177558-01-8
5-[3-(4-bromo-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-dibromo-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole

: 1177558-02-9
5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole

Guidance literature:: 3,5-bis-[4-(2-ethylhexyloxy)phenyl]-1-iodo-4-methylbenzene; With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 1.5h; Inert atmosphere;

With boric acid tributyl ester; In tetrahydrofuran; at -78 - 20 ℃; for 66h;

5-[3-(4-bromo-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-dibromo-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole; Further stages;
DOI:10.1021/ja903157e

Reference yield: 64.0%

: iridium(III) chloride trihydrate

: 1177558-02-9
5-[3-(4-{3,5-bis[4-(2-ethylhexyloxy)phenyl]-4-methylphenyl}-2,5-dimethylphenyl)-4-fluorophenyl]-1-[3,5-bis(3,5-bis{4-[2-ethylhexyloxy]phenyl}-4-methylphenyl)-4-methylbenzyl]-3-propyl-1H-[1,2,4]triazole

: Ir⁽³⁺⁾*3C₂N₃(C₃H₇)(C₆H₂FC₆H₂(CH₃)2C₆H₂CH₃(C₆H₄OC₈H₁₇)2)(CH₂C₆H₂CH₃(C₆H₂CH₃(C₆H₄OC₈H₁₇)2)2)^(1-)=C₃₉₆H₄₉₅F₃IrN₉O₁₈

Guidance literature:: With silver trifluoromethanesulfonate; In H₂O; further solvent(s); 1. IrCl3*3H2O, water, 2-(n-butoxy)ethanol, heating at reflux under Ar, then AgOSO2CF3, an excess of triazole-compound, diglyme, heat, Ar; column chromy.;
DOI:10.1021/ja903157e