(η-triphenylcyclopropenyl)dicarbonyltris(acetonitrile)molybdenum(1+) hexafluorophosphate

Base Information

Chemical Name:(η-triphenylcyclopropenyl)dicarbonyltris(acetonitrile)molybdenum(1+) hexafluorophosphate
CAS No.:97689-41-3
Molecular Formula:C₂₉H₂₄MoN₃O₂*F₆P
Molecular Weight:687.433
Hs Code.:

Synonyms:(η-triphenylcyclopropenyl)dicarbonyltris(acetonitrile)molybdenum(1+) hexafluorophosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η-triphenylcyclopropenyl)dicarbonyltris(acetonitrile)molybdenum(1+) hexafluorophosphate

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Technology Process of (η-triphenylcyclopropenyl)dicarbonyltris(acetonitrile)molybdenum(1+) hexafluorophosphate

There total 1 articles about (η-triphenylcyclopropenyl)dicarbonyltris(acetonitrile)molybdenum(1+) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: triphenylcyclopropenylium hexafluorophosphate

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 97689-41-3
(η-triphenylcyclopropenyl)dicarbonyltris(acetonitrile)molybdenum(1+) hexafluorophosphate

Guidance literature:: With CH₃CN; In acetonitrile; Mo(CO)6 refluxing in MeCN for 4 h under N2, cooling to room temp., PF6 salt adding, heating at 65°C overnight, cooling, solvent removingin vacuo; purified by recrystallization from CH2Cl2-ether; identified by elem. anal., IR and NMR spectra;

Reference yield: 93.0%

: 97689-41-3
(η-triphenylcyclopropenyl)dicarbonyltris(acetonitrile)molybdenum(1+) hexafluorophosphate

: cyclopentadienylthallium(I)

: 82661-45-8
(η-cyclopentadienyl)(η-triphenylcyclopropenyl)dicarbonylmolybdenum

Guidance literature:: In tetrahydrofuran; C5H5Tl adding to a soln. of the complex under N2, stirring at room temp. overnight; purified by chromy. on Florisil at -20°C and recrystallization from hexane; identified by elem. anal., IR, NMR spectra and a single crystal X-ray diffraction;