methyl (methyl 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Base Information

• Chemical Name: methyl (methyl 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate
• CAS No.: 6730-26-3
• Molecular Formula: C₁₃H₂₃NO₉
• Molecular Weight: 337.327
• Mol file: 6730-26-3.mol

Synonyms:methyl (methyl 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Chemical Property of methyl (methyl 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl (methyl 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

There total 3 articles about methyl (methyl 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Methyl-4,7,8,9-tetra-O-acetyl-5-acetylamino-3,5-didesoxy-β-L-glycero-D-galacto-2-nonulopyranosidonsaeuremethylester (99395-95-6) → Methyl-5-acetylamino-3,5-didesoxy-β-L-glycero-D-galacto-2-nonulopyranosidonsaeuremethylester (6730-26-3,6730-43-4,99336-20-6,140195-54-6)

Guidance literature:

With sodium methylate; In methanol; for 1h; Ambient temperature;

DOI:10.1007/BF00798282

Reference yield:

Methyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-L-glycero-α-D-galacto-2-nonulopyranosidonsaeuremethylester (41521-03-3,56323-64-9,73208-80-7,88547-02-8,99395-95-6,99395-96-7,99395-97-8,140385-82-6,140385-83-7,140385-84-8) → methyl α-glycoside of D-neuraminic acid (6730-26-3,6730-43-4,99336-20-6,140195-54-6)

Guidance literature:

With sodium methylate;

DOI:10.1016/S0040-4039(01)82928-2

Reference yield:

→ Methoxy-ovin-sialinsaeure-methylester (6730-26-3,6730-43-4,99336-20-6,140195-54-6)

Guidance literature:

N-Acetyl-neuraminsaeure (Ovin-sialinsaeure) , sd. Me./Dowex 50;

upstream raw materials:

Methyl-4,7,8,9-tetra-O-acetyl-5-acetylamino-3,5-didesoxy-β-L-glycero-D-galacto-2-nonulopyranosidonsaeuremethylester

Methyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-L-glycero-α-D-galacto-2-nonulopyranosidonsaeuremethylester

Downstream raw materials:

Methyl-5-acetylamino-4,9-bis-O-(t-butyldimethylsilyl)-3,5-didesoxy-8-O-tosyl-β-L-glycero-D-galacto-2-nonulopyranosidonsaeuremethylester

Neu5AcαOMe

methyl [O-methyl-(5-acetamido-3,5-dideoxy-9-O-(4-toluenesulfonyl)-D-glycero-α-D-galacto-2-nonulopyranosyl)]nonate

methyl [2-methyl-5-acetamido-3,5-dideoxy-8,9-O-(p-methoxybenzylidene)-D-glycero-α-D-galacto-2-nonulopyranosid]onate