(2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

Base Information

Chemical Name:(2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt
CAS No.:1384457-47-9
Molecular Formula:C₈H₁₁N*C₁₃H₁₆O₃
Molecular Weight:341.45
Hs Code.:

Synonyms:(2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

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Chemical Property of (2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

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Technology Process of (2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

There total 4 articles about (2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: (2RS,3RS)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 1384457-47-9
(2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

: (2S,3S)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

Guidance literature:: In ethanol; tert-butyl methyl ether; at 10 ℃; Resolution of racemate;

Reference yield:

: 6099-04-3,17570-26-2
trans-3-methoxycinnamic acid

: 1384457-47-9
(2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

: (2S,3S)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / toluene / -15 - 20 °C / Inert atmosphere

1.2: Cooling with ice

2.1: carbon tetrabromide / 10 h / 60 °C

3.1: triethylamine; lithium hexamethyldisilazane / toluene / 2.83 h / -60 °C / Inert atmosphere

3.2: 0.17 h

3.3: Cooling with ice

4.1: ethanol; tert-butyl methyl ether / 10 °C / Resolution of racemate

With diisobutylaluminium hydride; triethylamine; lithium hexamethyldisilazane; carbon tetrabromide; In ethanol; tert-butyl methyl ether; toluene;

Reference yield:

: 125617-35-8
(E)-3-(3-Methoxyphenyl)-2-propen-1-ol

: 1384457-47-9
(2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

: (2S,3S)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: carbon tetrabromide / 10 h / 60 °C

2.1: triethylamine; lithium hexamethyldisilazane / toluene / 2.83 h / -60 °C / Inert atmosphere

2.2: 0.17 h

2.3: Cooling with ice

3.1: ethanol; tert-butyl methyl ether / 10 °C / Resolution of racemate

With triethylamine; lithium hexamethyldisilazane; carbon tetrabromide; In ethanol; tert-butyl methyl ether; toluene;