dimesitylphosphinic chloride

Base Information

• Chemical Name: dimesitylphosphinic chloride
• CAS No.: 31639-12-0
• Molecular Formula: C₁₈H₂₂ClOP
• Molecular Weight: 320.799
• Mol file: 31639-12-0.mol

Synonyms:dimesitylphosphinic chloride

Chemical Property of dimesitylphosphinic chloride

Chemical Property:

Purity/Quality:

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Technology Process of dimesitylphosphinic chloride

There total 4 articles about dimesitylphosphinic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

Bis(2,4,6-trimethylphenyl)phosphine oxide (23897-16-7) → dimesitylphosphinic chloride (31639-12-0)

Guidance literature:

With triethylamine; In tetrachloromethane; at 0 - 20 ℃; for 48h; Inert atmosphere;

DOI:10.1039/d0cc02039g

Reference yield:

dimesitylphosphinic acid (1732-67-8) → dimesitylphosphinic chloride (31639-12-0)

Guidance literature:

With thionyl chloride; for 2h; Heating;

Reference yield:

2-mesitylmagnesium bromide (2633-66-1) → dimesitylphosphinic chloride (31639-12-0)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorous oxychloride

2: thionyl chloride / 2 h / Heating

With thionyl chloride; trichlorophosphate;

upstream raw materials:

dimesitylphosphinic acid

2-mesitylmagnesium bromide

Bis(2,4,6-trimethylphenyl)phosphine oxide

Downstream raw materials:

dimesityl phosphine

dimesitylphosphinic amide

dimesitylphosphinic azide

methyl N,P-dimesitylphosphonamidate