dicyclohexyl[2-{5-(dicyclohexylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]phosphane

Base Information

Chemical Name:dicyclohexyl[2-{5-(dicyclohexylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]phosphane
CAS No.:1325745-95-6
Molecular Formula:C₃₇H₅₀F₂O₂P₂
Molecular Weight:626.747
Hs Code.:

Synonyms:dicyclohexyl[2-{5-(dicyclohexylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]phosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dicyclohexyl[2-{5-(dicyclohexylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]phosphane

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Technology Process of dicyclohexyl[2-{5-(dicyclohexylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]phosphane

There total 1 articles about dicyclohexyl[2-{5-(dicyclohexylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1300117-94-5
5-bromo-2,2-difluoro-4-(2-iodophenyl)benzo[d][1,3]dioxole

: 16523-54-9
chlorodicyclohexylphosphane

: 1325745-95-6
dicyclohexyl[2-{5-(dicyclohexylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]phosphane

Guidance literature:: 5-bromo-2,2-difluoro-4-(2-iodophenyl)benzo[d][1,3]dioxole; With n-butyllithium; In hexane; toluene; at 25 ℃; Inert atmosphere;

chlorodicyclohexylphosphane; In hexane; toluene; at 25 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejic.201100428