2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol

Base Information

Chemical Name:2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol
CAS No.:116953-32-3
Molecular Formula:C₃₈H₆₁NO₇S
Molecular Weight:675.971
Hs Code.:

Synonyms:2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol

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Chemical Property of 2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol

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Technology Process of 2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol

There total 3 articles about 2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98-59-9
p-toluenesulfonyl chloride

: 116953-31-2
2-O-benzyl-3-O-<(2-hydroxyethyl)carbamoyl>-1-O-octadecylglycerol

: 116953-32-3
2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol

Guidance literature:: With triethylamine; for 18h; Ambient temperature;
DOI:10.1021/jm00121a012

Reference yield:

: 86008-21-1,89104-47-2
2-(benzyloxy)-3-(octadecyloxy)-1-propanol

: 116953-32-3
2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 1.5 h / 0 °C

2: CHCl₃ / 21 h / Heating

3: 99 percent / Et₃N / 18 h / Ambient temperature

With pyridine; triethylamine; In dichloromethane; chloroform;
DOI:10.1021/jm00121a012

Reference yield:

: 116953-25-4
Carbonic acid 2-benzyloxy-3-octadecyloxy-propyl ester phenyl ester

: 116953-32-3
2-O-benzyl-1-O-octadecyl-3-O-<<2-<(p-toluenesulfonyl)oxy>ethyl>carbamoyl>glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 21 h / Heating

2: 99 percent / Et₃N / 18 h / Ambient temperature

With triethylamine; In chloroform;
DOI:10.1021/jm00121a012