2-Phenylethyl 2-cyclohexenyl sulfite

Base Information

• Chemical Name: 2-Phenylethyl 2-cyclohexenyl sulfite
• CAS No.: 125452-80-4
• Molecular Formula: C₁₄H₁₈O₃S
• Molecular Weight: 266.361

Synonyms:2-Phenylethyl 2-cyclohexenyl sulfite

Chemical Property of 2-Phenylethyl 2-cyclohexenyl sulfite

Chemical Property:

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Technology Process of 2-Phenylethyl 2-cyclohexenyl sulfite

There total 1 articles about 2-Phenylethyl 2-cyclohexenyl sulfite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Phenylethyl chlorosulfite (33681-75-3) + Cyclohex-2-enol (822-67-3) → 2-Phenylethyl 2-cyclohexenyl sulfite (125452-80-4)

Guidance literature:

With n-butyllithium; Multistep reaction; 1) THF, -78 deg C, 10 min; 2) 1 h,;

DOI:10.1021/jo00293a028

Reference yield: 63.0%

2-Phenylethyl 2-cyclohexenyl sulfite (125452-80-4) → 2'-Phenylethyl 2-cyclohexenesulfonate (125452-87-1)

Guidance literature:

[Pd₂(dba)₃]*benzene; triethyl phosphite; In 1,4-dioxane; for 26h; Ambient temperature;

DOI:10.1021/jo00293a028

upstream raw materials:

2-Phenylethyl chlorosulfite

Cyclohex-2-enol

Downstream raw materials:

2'-Phenylethyl 2-cyclohexenesulfonate

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