C₂₆H₂₈N₂O₄

Base Information

Chemical Name:C₂₆H₂₈N₂O₄
CAS No.:1419075-34-5
Molecular Formula:C₂₆H₂₈N₂O₄
Molecular Weight:432.519
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₆H₂₈N₂O₄

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Chemical Property of C₂₆H₂₈N₂O₄

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Technology Process of C₂₆H₂₈N₂O₄

There total 14 articles about C₂₆H₂₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₂₉H₃₄N₂O₅

: 1419075-34-5
C₂₆H₂₈N₂O₄

Guidance literature:: With hydrogenchloride; In acetone; at 20 ℃; for 96h;
DOI:10.1002/ejoc.201200919

Reference yield: 35.0%

: 1419075-27-6
C₂₉H₃₆N₂O₆

: C₂₉H₃₄N₂O₅

: 1419075-34-5
C₂₆H₂₈N₂O₄

: 1419075-35-6
C₂₆H₂₈N₂O₄

Guidance literature:: With methanesulfonic acid; In dichloromethane; for 1.5h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201200919

Reference yield:

: 1350922-84-7
(R)-benzyl [1-(2-(2-aminoethyl)-1,3-dioxan-2-yl)propan-2-yl]carbamate

: 1419075-34-5
C₂₆H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

1.2: 0.5 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; ammonium formate / methanol / 3 h / Reflux

3.1: magnesium sulfate / dichloromethane / Reflux

3.2: 14 h / 40 °C

4.1: palladium 10% on activated carbon; ammonium formate / methanol / 2 h / Reflux

5.1: sodium carbonate / dichloromethane; water / 3 h / 20 °C

6.1: Amberlite IRA 401 / methanol

7.1: triethylamine / toluene / 3 h / Dean-Stark; Reflux

8.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.5 h / -20 - 5 °C / Inert atmosphere

9.1: methanesulfonic acid / dichloromethane / 1.5 h / Inert atmosphere

10.1: hydrogenchloride / acetone / 96 h / 20 °C

With hydrogenchloride; dmap; sodium tetrahydroborate; methanesulfonic acid; palladium 10% on activated carbon; ammonium formate; sodium carbonate; magnesium sulfate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene; 3.1: |Mannich Aminomethylation;
DOI:10.1002/ejoc.201200919