C₂₆H₂₈N₄O₃

Base Information

Chemical Name:C₂₆H₂₈N₄O₃
CAS No.:1431701-31-3
Molecular Formula:C₂₆H₂₈N₄O₃
Molecular Weight:444.533
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₂₆H₂₈N₄O₃

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Chemical Property of C₂₆H₂₈N₄O₃

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Technology Process of C₂₆H₂₈N₄O₃

There total 7 articles about C₂₆H₂₈N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1431703-32-0
C₃₂H₄₂N₄O₃Si

: 1431701-31-3
C₂₆H₂₈N₄O₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 1431701-05-1
C₂₄H₂₄N₄O₂

: 1431701-31-3
C₂₆H₂₈N₄O₃

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil; tetrahydrofuran / 0 °C / Sealed tube; Reflux

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; mineral oil;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1431701-31-3
C₂₆H₂₈N₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 4 h / 100 °C / Inert atmosphere

5.1: sodium hydride / mineral oil; tetrahydrofuran / 0 °C / Sealed tube; Reflux

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; palladium diacetate; sodium hydride; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;