(2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex

Base Information

Chemical Name:(2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex
CAS No.:1204221-51-1
Molecular Formula:C₉H₁₁NO₂*C₂₂H₂₅ClO₅
Molecular Weight:572.066
Hs Code.:

Synonyms:(2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex

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Chemical Property of (2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex

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Technology Process of (2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex

There total 7 articles about (2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1204220-75-6
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

: 1204221-51-1
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex

Guidance literature:: In ethanol; water; at 80 ℃;

Reference yield:

: 1204220-70-1
(5-bromo-2-chlorophenyl)(4-cyclopropylphenyl)methanone

: 1204221-51-1
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex

Guidance literature:: Multi-step reaction with 4 steps

1.1: Et₃SiD; trifluorormethanesulfonic acid; trifluoroacetic acid / tetrahydrofuran / 2 h / 25 °C

2.1: n-butyllithium / tetrahydrofuran; hexane; toluene / -60 °C / Inert atmosphere

2.2: -55 - 60 °C

2.3: 20 °C

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -40 - 20 °C

4.1: ethanol; water / 80 °C

With triethylsilane; n-butyllithium; Et₃SiD; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; trifluoroacetic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 1204220-77-8
4-bromo-1-chloro-2-(4-cyclopropylbenzyl)benzene

: 1204221-51-1
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol, L-phenylalanine complex

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutylammonium bisulfate; water-d2; sodium hydride / hexane / 0 - 25 °C

1.2: 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane; toluene / -60 °C / Inert atmosphere

2.2: -55 - 60 °C

2.3: 20 °C

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -40 - 20 °C

4.1: ethanol; water / 80 °C

With triethylsilane; n-butyllithium; tetrabutylammonium bisulfate; boron trifluoride diethyl etherate; water-d2; sodium hydride; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene; acetonitrile;