Technology Process of C27H40O3
There total 7 articles about C27H40O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
platinum;
In
ethanol;
under 760 Torr;
Yield given;
Ambient temperature;
DOI:10.1021/ja00405a069
-
-
79243-44-0
(4bS,7S,8aR,10aS)-7-Benzyloxy-2,4b,8,8-tetramethyl-1,4b,5,6,7,8,8a,9,10,10a-decahydro-2H-phenanthren-3-one
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) LiN3)2>2
2: aq. KOH / acetone / Heating
3: 21 percent / Pb(OAc)4, O2, pyridine / 90 °C
4: NaBH4 / ethanol / 25 °C
5: 77 percent / TsCl, pyridine / 40 °C
6: OsO4, pyridine / diethyl ether / -10 deg C -> room temperature
7: H2 / Pt black / ethanol / 760 Torr / Ambient temperature
With
pyridine; lead(IV) acetate; potassium hydroxide; sodium tetrahydroborate; osmium(VIII) oxide; hydrogen; oxygen; p-toluenesulfonyl chloride; lithium diisopropyl amide;
platinum;
In
diethyl ether; ethanol; acetone;
DOI:10.1021/ja00405a069
- Guidance literature:
-
Multi-step reaction with 2 steps
1: OsO4, pyridine / diethyl ether / -10 deg C -> room temperature
2: H2 / Pt black / ethanol / 760 Torr / Ambient temperature
With
pyridine; osmium(VIII) oxide; hydrogen;
platinum;
In
diethyl ether; ethanol;
DOI:10.1021/ja00405a069