(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br

Base Information

Chemical Name:(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br
CAS No.:15699-66-8
Molecular Formula:Br*C₅₃H₄₈IrOP₄
Molecular Weight:1096.98
Hs Code.:

(CO)Ir((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2<sup>(1+)</sup>*Br<sup>(1-)</sup>=[(CO)Ir((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2]Br

Synonyms:(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br

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Chemical Property of (CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br

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Technology Process of (CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br

There total 2 articles about (CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 15842-08-7
trans-IrBr(OC){P(C₆H₅)3}2

: 15699-66-8
(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: P(C₆H₅)3 / acetone

With P(C₆H₅)3; In tetrahydrofuran; acetone;
DOI:10.1021/ja00297a021

Reference yield:

: 29638-05-9
iridium(I)(Br)(carbonyl)(1,2-bis(diphenylphosphino)ethane)

: 15842-08-7
trans-IrBr(OC){P(C₆H₅)3}2

: 15699-66-8
(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br

Guidance literature:: With P(C₆H₅)3; In acetone; 1 equiv. of PPh3 was added to soln. of Ir complex in acetone, reacted for 20 min; monitored by IR;
DOI:10.1021/ja00297a021

Reference yield: 20.0%

: 15699-66-8
(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=[(CO)Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]Br

: nitrosonium tetrafluoroborate

: 91685-27-7
trans-[IrBr(CO)(1,2-bis(diphenylphosphino)ethane)2][BF₄]2

Guidance literature:: In acetonitrile; complex soln. satd. with CO added to solid NOBF4, stirred for 0.5 h; pptd. (ether), filtered, ppt. discarded, pptd. (ether), ppt. recrystd. (CH2Cl2/Et2O); elem. anal.;