C₂₅H₃₀O₃

Base Information Edit

Chemical Name:C₂₅H₃₀O₃
CAS No.:325142-45-8
Molecular Formula:C₂₅H₃₀O₃
Molecular Weight:378.511
Hs Code.:
Mol file:325142-45-8.mol

C<sub>25</sub>H<sub>30</sub>O<sub>3</sub>

Synonyms:C₂₅H₃₀O₃

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Chemical Property of C₂₅H₃₀O₃ Edit

Chemical Property:

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Technology Process of C₂₅H₃₀O₃

There total 9 articles about C₂₅H₃₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 325142-44-7
C₂₇H₃₃BrO₄

: 325142-45-8
C₂₅H₃₀O₃

Guidance literature:: With acetic acid; zinc; In ethanol; Heating;
DOI:10.1021/ol006922o

Reference yield:

: 325142-36-7
(3aR,4R,7S,7aR)-2-Hydroxymethyl-3a,4,7,7a-tetrahydro-4,7-methano-inden-1-one

: 325142-45-8
C₂₅H₃₀O₃

Guidance literature:: Multi-step reaction with 10 steps

1: DIBAL

2: 99 percent / NBS / CH₂Cl₂ / 0 °C

3: 87 percent / diphenyl ether / Heating

4: 75 percent / LDA / tetrahydrofuran / -78 °C

5: 66 percent / DMSO / CH₂Cl₂ / Heating

6: 94 percent / tetrahydrofuran / -20 °C

7: p-TsOH

8: 90 percent / Li(Et)3BH / tetrahydrofuran

9: 87 percent / NaH / tetrahydrofuran

10: 85 percent / Zn; acetic acid / ethanol / Heating

With N-Bromosuccinimide; sodium hydride; diisobutylaluminium hydride; lithium triethylborohydride; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; zinc; lithium diisopropyl amide; In tetrahydrofuran; diphenylether; ethanol; dichloromethane; 3: Eschenmoser rearrangement / 5: Pauson-Khand reaction;
DOI:10.1021/ol006922o

Reference yield:

: 244616-79-3
(1R,3aR,4R,7S,7aR)-2-Hydroxymethyl-3a,4,7,7a-tetrahydro-1H-4,7-methano-inden-1-ol

: 325142-45-8
C₂₅H₃₀O₃

Guidance literature:: Multi-step reaction with 9 steps

1: 99 percent / NBS / CH₂Cl₂ / 0 °C

2: 87 percent / diphenyl ether / Heating

3: 75 percent / LDA / tetrahydrofuran / -78 °C

4: 66 percent / DMSO / CH₂Cl₂ / Heating

5: 94 percent / tetrahydrofuran / -20 °C

6: p-TsOH

7: 90 percent / Li(Et)3BH / tetrahydrofuran

8: 87 percent / NaH / tetrahydrofuran

9: 85 percent / Zn; acetic acid / ethanol / Heating

With N-Bromosuccinimide; sodium hydride; lithium triethylborohydride; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; zinc; lithium diisopropyl amide; In tetrahydrofuran; diphenylether; ethanol; dichloromethane; 2: Eschenmoser rearrangement / 4: Pauson-Khand reaction;
DOI:10.1021/ol006922o