2-bromomethyl-4-(trifluoromethylsulfonyl)phenylboronic acid pinacol ester

Base Information

• Chemical Name: 2-bromomethyl-4-(trifluoromethylsulfonyl)phenylboronic acid pinacol ester
• CAS No.: 1030832-31-5
• Molecular Formula: C₁₄H₁₇BBrF₃O₄S
• Molecular Weight: 429.063

Synonyms:2-bromomethyl-4-(trifluoromethylsulfonyl)phenylboronic acid pinacol ester

Chemical Property of 2-bromomethyl-4-(trifluoromethylsulfonyl)phenylboronic acid pinacol ester

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Technology Process of 2-bromomethyl-4-(trifluoromethylsulfonyl)phenylboronic acid pinacol ester

There total 1 articles about 2-bromomethyl-4-(trifluoromethylsulfonyl)phenylboronic acid pinacol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4,4,5,5-tetramethyl-2-[2-methyl-4-(trifluoromethylsulfonyl)phenyl]-1,3,2-dioxaborolane (1011460-70-0) → 2-bromomethyl-4-(trifluoromethylsulfonyl)phenylboronic acid pinacol ester (1030832-31-5) + C14H16BBr2F3O4S

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 5h; Heating / reflux; Irradiation;

Reference yield: 95.0%

2-bromomethyl-4-(trifluoromethylsulfonyl)phenylboronic acid pinacol ester (1030832-31-5) + 9-[N-[3-(methacrylamido)propylamino]methyl]-10-[N-[2-(tert-butoxycarbonyl)ethylamino]methyl]-anthracene (1030832-19-9) → 9-[N-[6-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolano)-3-(trifluoromethylsulfonyl)benzyl]-N-[3-(methacrylamido)propylamino]methyl]-10-[N-[6-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolano)-3-(trifluoromethylsulfonyl)benzyl]-N-[2-(tert-butoxycarbonyl)ethylamino]methyl]anthracene (1030832-32-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 26h;

upstream raw materials:

4,4,5,5-tetramethyl-2-[2-methyl-4-(trifluoromethylsulfonyl)phenyl]-1,3,2-dioxaborolane

Downstream raw materials:

9-[N-[6-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolano)-3-(trifluoromethylsulfonyl)benzyl]-N-[3-(methacrylamido)propylamino]methyl]-10-[N-[6-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolano)-3-(trifluoromethylsulfonyl)benzyl]-N-[2-(tert-butoxycarbonyl)ethylamino]methyl]anthracene

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