5-{(E)-3-[3-(4-tert-butyl-diphenyl-silyloxy-1.5-dimethyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-1,3-bis(tert-butyl-dimethylsilyloxy)-cyclohexane

Base Information

• Chemical Name: 5-{(E)-3-[3-(4-tert-butyl-diphenyl-silyloxy-1.5-dimethyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-1,3-bis(tert-butyl-dimethylsilyloxy)-cyclohexane
• CAS No.: 882694-15-7
• Molecular Formula: C₅₃H₉₀O₃Si₃
• Molecular Weight: 859.552

Synonyms:5-{(E)-3-[3-(4-tert-butyl-diphenyl-silyloxy-1.5-dimethyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-1,3-bis(tert-butyl-dimethylsilyloxy)-cyclohexane

Chemical Property of 5-{(E)-3-[3-(4-tert-butyl-diphenyl-silyloxy-1.5-dimethyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-1,3-bis(tert-butyl-dimethylsilyloxy)-cyclohexane

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Technology Process of 5-{(E)-3-[3-(4-tert-butyl-diphenyl-silyloxy-1.5-dimethyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-1,3-bis(tert-butyl-dimethylsilyloxy)-cyclohexane

There total 1 articles about 5-{(E)-3-[3-(4-tert-butyl-diphenyl-silyloxy-1.5-dimethyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-1,3-bis(tert-butyl-dimethylsilyloxy)-cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1R,3R)-(3-((1S,4R)-4-(tert-butyl-diphenyl-silyloxy)-1,5-dimethylhexyl)-2,2,3-trimethyl)cyclopentane carbaldehyde (882694-14-6) + (1R,3R)-1,3-bis((tert-butyldimethyl)silanyloxy)-5-[2-(diphenylphosphinoyl)-ethylidene]cyclohexane (139356-39-1) → 5-{(E)-3-[3-(4-tert-butyl-diphenyl-silyloxy-1.5-dimethyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-1,3-bis(tert-butyl-dimethylsilyloxy)-cyclohexane (882694-15-7)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h;

Reference yield: 44.0%

5-{(E)-3-[3-(4-tert-butyl-diphenyl-silyloxy-1.5-dimethyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-1,3-bis(tert-butyl-dimethylsilyloxy)-cyclohexane (882694-15-7) → (1R,3R)-5-{(E)-3-[(S)-3-((R)-4-hydroxy-1-(S)-methyl-5-methyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-cyclohexane-1,3-diol (882694-16-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 12h;

upstream raw materials:

(1R,3R)-(3-((1S,4R)-4-(tert-butyl-diphenyl-silyloxy)-1,5-dimethylhexyl)-2,2,3-trimethyl)cyclopentane carbaldehyde

(1R,3R)-1,3-bis((tert-butyldimethyl)silanyloxy)-5-[2-(diphenylphosphinoyl)-ethylidene]cyclohexane

Downstream raw materials:

(1R,3R)-5-{(E)-3-[(S)-3-((R)-4-hydroxy-1-(S)-methyl-5-methyl-hexyl)-2,2,3-trimethyl-cyclopentyl]-allylidene}-cyclohexane-1,3-diol

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