Technology Process of C28H40O8
There total 12 articles about C28H40O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
at 20 ℃;
for 2h;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 0.13 h / 20 °C / pH 7.2 / Inert atmosphere
2.1: pyridine hydrogenfluoride / tetrahydrofuran / 22 h / 4 °C / Cooling
3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C
3.2: 3.5 h / 20 °C
4.1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 20 °C
With
potassium permanganate; sodium periodate; 2,4,6-trichlorobenzoyl chloride; palladium 10% on activated carbon; hydrogen; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; aq. phosphate buffer; ethanol; toluene; tert-butyl alcohol;
3.1: |Yamaguchi Lactonization / 3.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C
1.2: 3.5 h / 20 °C
2.1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 20 °C
With
2,4,6-trichlorobenzoyl chloride; palladium 10% on activated carbon; hydrogen; triethylamine;
In
ethanol; toluene;
1.1: |Yamaguchi Lactonization / 1.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008
