1-PYRIDIN-2-YL-ETHANONE OXIME TOSYLATE

Base Information

• Chemical Name: 1-PYRIDIN-2-YL-ETHANONE OXIME TOSYLATE
• CAS No.: 74209-50-0
• Molecular Formula: C14H14 N2 O3 S
• Molecular Weight: 290.34
• Hs Code.: 2933399090
• Mol file: 74209-50-0.mol

Synonyms:1-PYRIDIN-2-YL-ETHANONE OXIME TOSYLATE

Chemical Property of 1-PYRIDIN-2-YL-ETHANONE OXIME TOSYLATE

Chemical Property:

• Vapor Pressure: 1.36E-07mmHg at 25°C
• Refractive Index: 1.584
• Boiling Point: 441.9°C at 760 mmHg
• Flash Point: 221°C
• PSA: 77.00000
• Density: 1.23g/cm³
• LogP: 3.60030

Purity/Quality:

NLT 98% ^*data from raw suppliers

(E)-[1-(PYRIDIN-2-YL)ETHYLIDENE]AMINO-4-METHYLBENZENE-1-SULFONATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-PYRIDIN-2-YL-ETHANONE OXIME TOSYLATE

There total 3 articles about 1-PYRIDIN-2-YL-ETHANONE OXIME TOSYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-pyridin-2-yl-ethanone oxime (1758-54-9,79462-42-3,81563-77-1) + p-toluenesulfonyl chloride (98-59-9) → C14H14N2O3S (74209-50-0)

Guidance literature:

With pyridine; at 20 ℃; for 24h;

Reference yield:

2-acetylpyridine (1122-62-9) → C14H14N2O3S (74209-50-0)

Guidance literature:

Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride

2: pyridine

With hydroxylamine hydrochloride; In pyridine;

DOI:10.1039/c9nj00420c

Reference yield:

1-pyridin-2-yl-ethanone oxime (1758-54-9,79462-42-3,81563-77-1) + p-toluenesulfonyl chloride (98-59-9) → 1-[2]pyridyl-ethanone-[O-(toluene-4-sulfonyl)-oxime ] (74209-50-0)

Guidance literature:

With pyridine;

upstream raw materials:

1-pyridin-2-yl-ethanone oxime

p-toluenesulfonyl chloride

2-acetylpyridine

Downstream raw materials:

2-amino-1-[2]pyridyl-ethanone; monohydrochloride

2,2-diethoxy-2-(2-pyridyl)ethylamine

2,2-diethoxy-2-(2-pyridyl)ethylamine dihydrochloride

2-amino-1-[2]pyridyl-ethanone

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