(S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid

Base Information

Chemical Name:(S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid
CAS No.:84866-45-5
Molecular Formula:C₂HF₃O₂*C₂₄H₃₀N₂O₆S
Molecular Weight:588.602
Hs Code.:

Synonyms:(S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid

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Chemical Property of (S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid

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Technology Process of (S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid

There total 4 articles about (S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84866-43-3
Z(OMe)-Glu(OBzl)-Met(O)-OBzl

: 84866-45-5
(S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In various solvent(s); at 0 ℃; for 1h;
DOI:10.1248/cpb.30.3970

Reference yield:

: 23506-06-1
Z(OMe)-Glu(OBzl)-OH

: 84866-45-5
(S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / DCC, HOBT / tetrahydrofuran / 20 h / Ambient temperature; 1.) ice-bath, 2 h; 2.) room temp., 20 h

2: 95 percent / N-chlorosuccinimide / ethyl acetate; H₂O / 0.5 h / 0 °C

3: trifluoroacetic acid, anisole / various solvent(s) / 1 h / 0 °C

With N-chloro-succinimide; benzotriazol-1-ol; methoxybenzene; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1248/cpb.30.3970

Reference yield:

: 63649-07-0
methionine benzyl ester

: 84866-45-5
(S)-2-((S)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methanesulfinyl-butyric acid benzyl ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / DCC, HOBT / tetrahydrofuran / 20 h / Ambient temperature; 1.) ice-bath, 2 h; 2.) room temp., 20 h

2: 95 percent / N-chlorosuccinimide / ethyl acetate; H₂O / 0.5 h / 0 °C

3: trifluoroacetic acid, anisole / various solvent(s) / 1 h / 0 °C

With N-chloro-succinimide; benzotriazol-1-ol; methoxybenzene; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1248/cpb.30.3970