5,9-Cycloundecadien-2-yn-1-ol,7,7,10-trimethyl-,(5Z,9Z)-(9CI)

Base Information

Chemical Name:5,9-Cycloundecadien-2-yn-1-ol,7,7,10-trimethyl-,(5Z,9Z)-(9CI)
CAS No.:791810-20-3
Molecular Formula:C₁₄H₂₀O
Molecular Weight:204.312
Hs Code.:
Mol file:791810-20-3.mol

Synonyms:5,9-Cycloundecadien-2-yn-1-ol,7,7,10-trimethyl-,(5Z,9Z)-(9CI)

Suppliers and Price of 5,9-Cycloundecadien-2-yn-1-ol,7,7,10-trimethyl-,(5Z,9Z)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,9-Cycloundecadien-2-yn-1-ol,7,7,10-trimethyl-,(5Z,9Z)-(9CI)

Chemical Property:

PSA：20.23000
LogP:3.06330

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5,9-Cycloundecadien-2-yn-1-ol,7,7,10-trimethyl-,(5Z,9Z)-(9CI)

There total 42 articles about 5,9-Cycloundecadien-2-yn-1-ol,7,7,10-trimethyl-,(5Z,9Z)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 791810-18-9
(3E,7Z)-11-Iodo-3,6,6-trimethyl-undeca-3,7-dien-10-ynal

: 791810-01-0,791810-20-3
(3E,7Z)-3,6,6-trimethylcycloundeca-3,7-dien-10-yn-1-ol

Guidance literature:: With chromium dichloride; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1021/ol048463n

Reference yield:

: 321852-67-9
(3E,7Z)-3,6,6-trimethylundeca-3,7-dien-10-yn-1-ol

: 791810-01-0,791810-20-3
(3E,7Z)-3,6,6-trimethylcycloundeca-3,7-dien-10-yn-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 989 mg / NIS; AgNO₃ / acetone / 4 h / 20 °C

2: 963 mg / 2-iodoxybenzoic acid / dimethylsulfoxide / 2 h / 20 °C

3: 269 mg / CrCl₂ / tetrahydrofuran / 12 h / 20 °C

With chromium dichloride; N-iodo-succinimide; silver nitrate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; acetone;
DOI:10.1021/ol048463n

Reference yield:

: 791810-17-8
(3E,7Z)-11-Iodo-3,6,6-trimethyl-undeca-3,7-dien-10-yn-1-ol

: 791810-01-0,791810-20-3
(3E,7Z)-3,6,6-trimethylcycloundeca-3,7-dien-10-yn-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 963 mg / 2-iodoxybenzoic acid / dimethylsulfoxide / 2 h / 20 °C

2: 269 mg / CrCl₂ / tetrahydrofuran / 12 h / 20 °C

With chromium dichloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ol048463n