4-hydroxyimino-1-methyl-2-phenethylhexahydropyridazine

Base Information

• Chemical Name: 4-hydroxyimino-1-methyl-2-phenethylhexahydropyridazine
• CAS No.: 172292-94-3
• Molecular Formula: C₁₃H₁₉N₃O
• Molecular Weight: 233.313
• Mol file: 172292-94-3.mol

Synonyms:4-hydroxyimino-1-methyl-2-phenethylhexahydropyridazine

Chemical Property of 4-hydroxyimino-1-methyl-2-phenethylhexahydropyridazine

Chemical Property:

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Technology Process of 4-hydroxyimino-1-methyl-2-phenethylhexahydropyridazine

There total 1 articles about 4-hydroxyimino-1-methyl-2-phenethylhexahydropyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1-methyl-2-phenethylhexahydropyridazin-4-one hydrochloride → 4-hydroxyimino-1-methyl-2-phenethylhexahydropyridazine (172292-94-3)

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; In methanol; for 0.5h;

DOI:10.1007/BF00698440

Reference yield:

4-hydroxyimino-1-methyl-2-phenethylhexahydropyridazine (172292-94-3) → 1-methyl-2-phenethyl-4-propionamidohexahydropyridazine

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / LiAlH₄ / diethyl ether / 6 h

2: 62 percent / Et₃N / benzene / 1 h / 40 °C

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; benzene;

DOI:10.1007/BF00698440