5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione

Base Information

• Chemical Name: 5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione
• CAS No.: 129012-69-7
• Molecular Formula: C₁₅H₂₃NO₄
• Molecular Weight: 281.352

Synonyms:5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione

Chemical Property of 5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione

Chemical Property:

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Technology Process of 5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione

There total 2 articles about 5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Isopropylideneaminooxy-butyric acid 5,5-dimethyl-3-oxo-cyclohex-1-enyl ester → 5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione (129012-69-7)

Guidance literature:

With dmap; In toluene; at 110 ℃; for 7h; Yield given;

DOI:10.1071/CH9900427

Reference yield:

4-(1'-methylethylideneaminooxy)butanoic acid (129012-68-6) → 5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione (129012-69-7)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / Ambient temperature

2: 4-(dimethylamino)pyridine / toluene / 7 h / 110 °C

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; toluene;

DOI:10.1071/CH9900427

Reference yield: 62.0%

5,5-dimethyl-2-<4'-(1''-methylethylideneaminooxy)butanoyl>cyclohexane-1,3-dione (129012-69-7) → 2-(5',6'-dihydro-4'H-1',2'-oxazin-3'-yl)-5,5-dimethylcyclohexane-1,3-dione (129012-66-4)

Guidance literature:

With girard's reagent P; In ethanol; acetic acid; at 70 ℃; for 1.25h;

DOI:10.1071/CH9900427

upstream raw materials:

4-(1'-methylethylideneaminooxy)butanoic acid

Downstream raw materials:

2-(5',6'-dihydro-4'H-1',2'-oxazin-3'-yl)-5,5-dimethylcyclohexane-1,3-dione

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