2,5-bis<<5-(benzyloxycarbonyl)-3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrol-2-yl>methyl>-3,4-diphenylpyrrole

Base Information

Chemical Name:2,5-bis<<5-(benzyloxycarbonyl)-3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrol-2-yl>methyl>-3,4-diphenylpyrrole
CAS No.:172959-69-2
Molecular Formula:C₅₂H₅₁N₃O₈
Molecular Weight:845.992
Hs Code.:

Synonyms:2,5-bis<<5-(benzyloxycarbonyl)-3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrol-2-yl>methyl>-3,4-diphenylpyrrole

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Chemical Property of 2,5-bis<<5-(benzyloxycarbonyl)-3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrol-2-yl>methyl>-3,4-diphenylpyrrole

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Technology Process of 2,5-bis<<5-(benzyloxycarbonyl)-3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrol-2-yl>methyl>-3,4-diphenylpyrrole

There total 1 articles about 2,5-bis<<5-(benzyloxycarbonyl)-3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrol-2-yl>methyl>-3,4-diphenylpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1632-48-0
3,4-diphenyl-1H-pyrrole

: 859-38-1
benzyl 5-acetoxymethyl-4-(2-methoxycarbonylethyl)-3-methylpyrrole-2-carboxylate

: 172959-69-2
2,5-bis<<5-(benzyloxycarbonyl)-3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrol-2-yl>methyl>-3,4-diphenylpyrrole

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 60 ℃; for 12h;
DOI:10.1021/jo951870f

Reference yield:

: 172959-69-2
2,5-bis<<5-(benzyloxycarbonyl)-3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrol-2-yl>methyl>-3,4-diphenylpyrrole

: 17,18-diethyl-3,12-bis<2-(methoxycarbonyl)ethyl>-2,13-dimethyl-7,8-diphenylporphyrin

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, H₂ / Pd-C / tetrahydrofuran / 10 h / Ambient temperature

2: 31 percent / K₃Fe(CN)6 / methanol / 6 h / Heating

With hydrogen; triethylamine; potassium hexacyanoferrate(III); palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jo951870f