C₂₈H₄₂O₅SSi

Base Information

Chemical Name:C₂₈H₄₂O₅SSi
CAS No.:1352496-74-2
Molecular Formula:C₂₈H₄₂O₅SSi
Molecular Weight:518.79
Hs Code.:

C<sub>28</sub>H<sub>42</sub>O<sub>5</sub>SSi

Synonyms:C₂₈H₄₂O₅SSi

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Chemical Property of C₂₈H₄₂O₅SSi

Chemical Property:

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Technology Process of C₂₈H₄₂O₅SSi

There total 7 articles about C₂₈H₄₂O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1352496-99-1
C₂₂H₂₈O₅S

: 69739-34-0
t-butyldimethylsiyl triflate

: 1352496-74-2
C₂₈H₄₂O₅SSi

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.011

Reference yield:

: 1352496-98-0
C₂₉H₃₁NO₈S

: 1352496-74-2
C₂₈H₄₂O₅SSi

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; potassium carbonate / 20 °C / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; methanol; potassium carbonate; In dichloromethane;
DOI:10.1016/j.tet.2011.09.011

Reference yield:

: 1352496-70-8
C₂₂H₂₆O₅S

: 1352496-74-2
C₂₈H₄₂O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1: samarium diiodide / tetrahydrofuran; methanol / 0 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 20 °C / Inert atmosphere

3: methanol; potassium carbonate / 20 °C / Inert atmosphere

4: 2,6-dimethylpyridine / dichloromethane / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; methanol; samarium diiodide; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; toluene; 2: Mitsunobu reaction;
DOI:10.1016/j.tet.2011.09.011