allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate

Base Information

Chemical Name:allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate
CAS No.:220784-30-5
Molecular Formula:C₆₃H₇₀N₂O₈
Molecular Weight:983.257
Hs Code.:

Synonyms:allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate

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Chemical Property of allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate

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Technology Process of allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate

There total 5 articles about allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 170117-45-0
allyl 10-(vinyloxy)decanoate

: 170117-46-1
(2S,3S,5S)-3-hydroxy-2,5-bis<(fluorenylmethyloxycarbonyl)amino>-1,6-diphenylhexane

: 220784-30-5
allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; for 1h;
DOI:10.1021/jm00016a001

Reference yield:

: 1679-53-4
10-hydroxydecanoic acid

: 220784-30-5
allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride, 4-(dimethylamino)pyridine / CH₂Cl₂ / 2 h

2: 61 percent / mercury acetate / Heating

3: 67 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 1 h

With dmap; mercury(II) diacetate; pyridinium p-toluenesulfonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/jm00016a001

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 220784-30-5
allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 84.2 percent / diisopropylethylamine / CH₂Cl₂ / Ambient temperature

2: 67 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 1 h

With pyridinium p-toluenesulfonate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm00016a001