C₄₅H₅₆N₆O₁₂

Base Information

Chemical Name:C₄₅H₅₆N₆O₁₂
CAS No.:1360603-28-6
Molecular Formula:C₄₅H₅₆N₆O₁₂
Molecular Weight:872.973
Hs Code.:

C<sub>45</sub>H<sub>56</sub>N<sub>6</sub>O<sub>12</sub>

Synonyms:C₄₅H₅₆N₆O₁₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₅H₅₆N₆O₁₂

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Technology Process of C₄₅H₅₆N₆O₁₂

There total 11 articles about C₄₅H₅₆N₆O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1360566-56-8
C₄₃H₅₄N₆O₁₁

: 108-24-7
acetic anhydride

: 1360603-28-6
C₄₅H₅₆N₆O₁₂

Guidance literature:: With pyridine; at 20 - 50 ℃; for 3h;
DOI:10.1002/chem.201101058

Reference yield:

: 1360566-51-3
C₂₄H₄₀N₂O₆Si

: 1360603-28-6
C₄₅H₅₆N₆O₁₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / -40 °C

1.2: 5 h / -40 - 0 °C

2.1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

3.1: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

4.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

5.1: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

7.1: 20 % Pd(OH)2/C; hydrogen / methanol / 3 h / 20 °C

8.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 2 h / 20 °C

9.1: pyridine / 3 h / 20 - 50 °C

With pyridine; hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; sodium acetate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058

Reference yield:

: 1221741-69-0
C₂₄H₄₂N₂O₅Si

: 1360603-28-6
C₄₅H₅₆N₆O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

2: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

3: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

6: 20 % Pd(OH)2/C; hydrogen / methanol / 3 h / 20 °C

7: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 2 h / 20 °C

8: pyridine / 3 h / 20 - 50 °C

With pyridine; hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; sodium acetate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058