CIS-1,4,8,11-PERHYDROTETRAAZAPYRENE

Base Information

• Chemical Name: CIS-1,4,8,11-PERHYDROTETRAAZAPYRENE
• CAS No.: 74199-16-9
• Molecular Formula: C12H22 N4
• Molecular Weight: 222.333
• Hs Code.: 2933998090
• Mol file: 74199-16-9.mol

Synonyms:CIS-1,4,8,11-PERHYDROTETRAAZAPYRENE;CYCLAM GLYOXAL;CYCLAN GLYOXAL;CIS-PTAP;DECAHYDRO-CIS-1H,6H-3A,5A,8A,10A-TETRAAZAPYRENE;Cyclan glyoxal, cis-PTAP;cis-PTAP, 98 %;cis-Decahydro-1H,6H-3a,5a,8a,10a-tetraazapyrene

Chemical Property of CIS-1,4,8,11-PERHYDROTETRAAZAPYRENE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 83 °C
• Refractive Index: 1.645
• Boiling Point: 357.241°C at 760 mmHg
• Flash Point: 155.493°C
• PSA: 30.54000
• Density: 1.241g/cm³
• LogP: -0.38800
• Sensitive.: Hygroscopic

Purity/Quality:

98%,99%, ^*data from raw suppliers

cis-Decahydro-1H,6H-3a,5a,8a,10a-tetraazapyrene >98.0%(GC) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CIS-1,4,8,11-PERHYDROTETRAAZAPYRENE

There total 4 articles about CIS-1,4,8,11-PERHYDROTETRAAZAPYRENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1,4,8,11-Tetraazacyclotetradecane (295-37-4) + Glyoxal (131543-46-9,107-22-2) → cis-4,7,11,14-tetraazaperhydropyrene (74199-16-9)

Guidance literature:

In methanol; water; at 20 ℃; for 3h;

DOI:10.1039/b103995b

Reference yield: 80.0%

(10bS,10cR)-Decahydro-3a,5a,8a,10a-tetraaza-pyrene-1,8-dione → cis-4,7,11,14-tetraazaperhydropyrene (74199-16-9)

Guidance literature:

With dimethylsulfide borane complex; In tetrahydrofuran; Heating;

DOI:10.1039/b109307j

Reference yield: 80.0%

(10bR,10cR)-Decahydro-3a,5a,8a,10a-tetraaza-pyrene-1,6-dione → cis-4,7,11,14-tetraazaperhydropyrene (74199-16-9)

Guidance literature:

With dimethylsulfide borane complex; In tetrahydrofuran; Heating;

DOI:10.1039/b109307j

upstream raw materials:

1,4,8,11-Tetraazacyclotetradecane

Glyoxal

Downstream raw materials:

4,11-bis(4-methylbenzyl)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane