C₃₉H₅₈O₇Si

Base Information

Chemical Name:C₃₉H₅₈O₇Si
CAS No.:1375412-60-4
Molecular Formula:C₃₉H₅₈O₇Si
Molecular Weight:666.971
Hs Code.:

C<sub>39</sub>H<sub>58</sub>O<sub>7</sub>Si

Synonyms:C₃₉H₅₈O₇Si

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Chemical Property of C₃₉H₅₈O₇Si

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Technology Process of C₃₉H₅₈O₇Si

There total 15 articles about C₃₉H₅₈O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1375412-54-6
C₄₅H₇₄O₆Si₂

: 1375412-60-4
C₃₉H₅₈O₇Si

Guidance literature:: With Jones reagent; In acetone; at 0 ℃; for 1h;
DOI:10.1002/anie.201108692

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 1375412-60-4
C₃₉H₅₈O₇Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

2.1: copper(l) iodide / tetrahydrofuran; dimethyl sulfate / 3 h / -30 °C

3.1: sodium periodate / tetrahydrofuran; water / 6 h / 20 °C

4.1: N-chloro-succinimide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / acetonitrile / 2.5 h / 0 °C

4.2: 0.5 h

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

5.2: 1 h / -50 - -45 °C

5.3: 2 h / -70 - 0 °C

6.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

7.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

8.1: dmap; 2,4,6-trichlorobenzoyl chloride; dihydropyrimidinone / toluene / 7 h / 0 - 20 °C / Inert atmosphere

9.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 1.5 h

10.1: Grela's catalyst; 2,3,5,6-tetrafluoro-1,4-benzoquinone / dichloromethane / 3 h / 60 °C / Inert atmosphere

10.2: 2 h / 20 °C

11.1: Jones reagent / acetone / 1 h / 0 °C

With 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; copper(l) iodide; Jones reagent; n-butyllithium; samarium diiodide; triphenyl-arsane; 2,3,5,6-tetrafluoro-1,4-benzoquinone; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; 2,4,6-trichlorobenzoyl chloride; Grela's catalyst; silver perchlorate; 3-chloro-benzenecarboperoxoic acid; dihydropyrimidinone; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; dimethyl sulfate; acetonitrile; 5.3: Brook rearrangement / 7.1: Evans-Tishchenko reduction / 9.1: Stille coupling;
DOI:10.1002/anie.201108692

Reference yield:

: 37715-31-4
(E)-5-(3,3-dimethyloxiran-2-yl)-3-methylpent-2-enyl acetate

: 1375412-60-4
C₃₉H₅₈O₇Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: copper(l) iodide / tetrahydrofuran; dimethyl sulfate / 3 h / -30 °C

2.1: sodium periodate / tetrahydrofuran; water / 6 h / 20 °C

3.1: N-chloro-succinimide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / acetonitrile / 2.5 h / 0 °C

3.2: 0.5 h

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

4.2: 1 h / -50 - -45 °C

4.3: 2 h / -70 - 0 °C

5.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

6.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

7.1: dmap; 2,4,6-trichlorobenzoyl chloride; dihydropyrimidinone / toluene / 7 h / 0 - 20 °C / Inert atmosphere

8.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 1.5 h

9.1: Grela's catalyst; 2,3,5,6-tetrafluoro-1,4-benzoquinone / dichloromethane / 3 h / 60 °C / Inert atmosphere

9.2: 2 h / 20 °C

10.1: Jones reagent / acetone / 1 h / 0 °C

With 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; copper(l) iodide; Jones reagent; n-butyllithium; samarium diiodide; triphenyl-arsane; 2,3,5,6-tetrafluoro-1,4-benzoquinone; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; 2,4,6-trichlorobenzoyl chloride; Grela's catalyst; silver perchlorate; dihydropyrimidinone; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; dimethyl sulfate; acetonitrile; 4.3: Brook rearrangement / 6.1: Evans-Tishchenko reduction / 8.1: Stille coupling;
DOI:10.1002/anie.201108692