sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate

Base Information

Chemical Name:sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate
CAS No.:1097934-94-5
Molecular Formula:C₁₃H₁₀Cl₂O₆PS*Na
Molecular Weight:419.154
Hs Code.:

Synonyms:sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate

Chemical Property:

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Technology Process of sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate

There total 7 articles about sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1097934-44-5
C₁₃H₁₁Cl₂O₆PS

: 1097934-94-5
sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 2h;
DOI:10.1080/10426507.2012.717147

Reference yield:

: O,O-dimethyl (2,4-dichlorophenoxyacetoxy)(thien-2-yl)methylphosphonate

: 1097934-94-5
sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium iodide / acetonitrile / 2 h / 30 °C / Inert atmosphere; Darkness

2: methanol / 30 °C

3: sodium hydroxide / methanol / 2 h / 20 °C

With methanol; sodium iodide; sodium hydroxide; In methanol; acetonitrile;
DOI:10.1080/10426507.2012.717147

Reference yield:

: 98335-90-1
dimethyl α-hydroxy-α-(2-thienyl)methanephosphonate

: 1097934-94-5
sodium hydrogen (1-{[2-(2,4-dichlorophenoxy)acetyl]oxy}-1-(thien-2-yl)methyl)phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 4 h / 5 °C

2: sodium iodide / acetonitrile / 2 h / 30 °C / Inert atmosphere; Darkness

3: methanol / 30 °C

4: sodium hydroxide / methanol / 2 h / 20 °C

With pyridine; methanol; sodium iodide; sodium hydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1080/10426507.2012.717147