5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione

Base Information

Chemical Name:5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione
CAS No.:1355250-54-2
Molecular Formula:C₄₇H₃₉ClN₄O₈
Molecular Weight:823.302
Hs Code.:

Synonyms:5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione

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Chemical Property of 5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione

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Technology Process of 5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione

There total 3 articles about 5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2-(4-chlorophenyl)-1,3-di(3-methyl-4-nitroisoxazol-5-yl)propane

: 94-41-7
benzalacetophenone

: 1355250-54-2
5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione

Guidance literature:: With piperidine; In ethanol; for 4h; Reflux;
DOI:10.1016/j.bmcl.2011.11.044

Reference yield:

: 51978-97-3,53557-97-4
3-methyl-4-nitro-5-(4-chlorostyryl)isoxazole

: 1355250-54-2
5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 1 h / Reflux

2: piperidine / ethanol / 4 h / Reflux

With piperidine; In ethanol;
DOI:10.1016/j.bmcl.2011.11.044

Reference yield:

: 1123-49-5
3,5-dimethyl-4-nitroisoxazole

: 1355250-54-2
5-(4-chlorophenyl)-4,6-di-(3-methyl-4-nitro-5-isoxazolyl)-1,3,7,9-tetraphenyl-1,9-nonanedione

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 1 h / Reflux

2: piperidine / ethanol / 4 h / Reflux

With piperidine; In ethanol;
DOI:10.1016/j.bmcl.2011.11.044