6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid

Base Information

• Chemical Name: 6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid
• CAS No.: 23112-67-6
• Molecular Formula: C₁₈H₁₅NO₅
• Molecular Weight: 325.321
• Mol file: 23112-67-6.mol

Synonyms:6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid

Chemical Property of 6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid

There total 1 articles about 6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid (23112-67-6)

Guidance literature:

entspr. Ethylester II;

Reference yield: 83.0%

4-fluoro-1-iodobenzene (352-34-1) + 6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid (23112-67-6) → C23H18FNO3 (1361247-74-6)

Guidance literature:

With silver carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium(II) bromide; In N,N-dimethyl acetamide; toluene; at 150 ℃; for 1h; Microwave irradiation; Inert atmosphere;

DOI:10.1021/ol300235k

Reference yield: 72.0%

3-bromo-6-methyl-2H-chromen-2-one (20875-75-6) + 6-methoxy-1-(4-methoxyphenyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid (23112-67-6) → 6-methoxy-1-(4-methoxyphenyl)-3-(6-methyl-2-oxo-2H-chromen-3-yl)quinolin-4(1H)-one

Guidance literature:

With silver carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium(II) bromide; In dimethyl sulfoxide; at 150 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;

DOI:10.1021/acs.joc.5b02103

Downstream raw materials:

C₂₃H₁₈FNO₃

C₂₇H₂₁NO₃