(R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol

Base Information

• Chemical Name: (R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol
• CAS No.: 16549-85-2
• Molecular Formula: C₃₀H₃₅NO₄
• Molecular Weight: 473.612

Synonyms:(R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol

Chemical Property of (R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol

Chemical Property:

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Technology Process of (R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol

There total 1 articles about (R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,5α-epoxy-19anti-((R)-1-hydroxy-1-methyl-3-phenyl-propyl)-3,6-dimethoxy-6β,14-ethano-morphin-7-ene-17-carbonitrile (16549-84-1) → (R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol (16549-85-2)

Guidance literature:

With potassium hydroxide; In diethylene glycol;

DOI:10.1021/ja00989a032

Reference yield:

(R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol (16549-85-2) → (2R,2'R)-4,4'-diphenyl-2,2'-[4,5α;4',5'α-diepoxy-3,6,3',6'-tetramethoxy-17,17'-methanediyl-bis-(6α,14α-etheno-morphinan-7α-yl)]-bis-butan-2-ol (16620-48-7,16659-03-3)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol

2: ethanol

In ethanol;

DOI:10.1021/ja00989a032

Reference yield:

(R)-2-(4,5α-epoxy-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol (16549-85-2) → (R)-2-{4,5α-epoxy-17-[4,5α-epoxy-19anti-(1-hydroxy-1-methyl-ethyl)-3,6-dimethoxy-6β,14-ethano-morphin-7-en-17-ylmethyl]-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl}-4-phenyl-butan-2-ol (16659-04-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol

2: ethanol

In ethanol;

DOI:10.1021/ja00989a032

upstream raw materials:

4,5α-epoxy-19anti-((R)-1-hydroxy-1-methyl-3-phenyl-propyl)-3,6-dimethoxy-6β,14-ethano-morphin-7-ene-17-carbonitrile

Downstream raw materials:

(R)-2-{4,5α-epoxy-17-[4,5α-epoxy-19anti-(1-hydroxy-1-methyl-ethyl)-3,6-dimethoxy-6β,14-ethano-morphin-7-en-17-ylmethyl]-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl}-4-phenyl-butan-2-ol

(R)-2-(4,5α-epoxy-17-hydroxymethyl-3,6-dimethoxy-6α,14α-etheno-morphinan-7α-yl)-4-phenyl-butan-2-ol

(2R,2'R)-4,4'-diphenyl-2,2'-[4,5α;4',5'α-diepoxy-3,6,3',6'-tetramethoxy-17,17'-methanediyl-bis-(6α,14α-etheno-morphinan-7α-yl)]-bis-butan-2-ol

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